[1]曾涛,周义凯,张坤,等. SiC/SiC陶瓷基复合材料SLS/PIP制备工艺及弯曲性能[J].哈尔滨理工大学学报,2020,25(03):163-168.[doi:10.15938/j.jhust.2020.03.025]
 ZENG Tao,ZHOU Yi kai,ZHANG Kun,et al. Fabrication and Mechanical Property of SiC/SiC Composites by Selective Laser Sintering Technology Combined with Precursor Impregnation and Pyrolysis Process[J].哈尔滨理工大学学报,2020,25(03):163-168.[doi:10.15938/j.jhust.2020.03.025]
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 SiC/SiC陶瓷基复合材料SLS/PIP制备工艺及弯曲性能()
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《哈尔滨理工大学学报》[ISSN:1007-2683/CN:23-1404/N]

卷:
25
期数:
2020年03期
页码:
163-168
栏目:
材料科学与工程
出版日期:
2020-06-25

文章信息/Info

Title:
 Fabrication and Mechanical Property of SiC/SiC Composites 
by Selective Laser Sintering Technology Combined 
with Precursor Impregnation and Pyrolysis Process
文章编号:
1007-2683(2020)03-0163-06
作者:
 曾涛1周义凯2张坤12余四文12
 1.哈尔滨理工大学 建筑工程学院,哈尔滨 150080;
2.哈尔滨理工大学 材料科学与工程学院,哈尔滨 150080)
Author(s):
 ZENG Tao1ZHOU Yikai2ZHANG Kun12YU Siwen12
 (1.School of Civil Engineering and Architecture, Harbin University of Science and Technology, Harbin 150080, China;
2.School of Material Science and Engineering, Harbin University of Science and Technology, Harbin 150080, China)
关键词:
 关键词:增材制造陶瓷基复合材料选择性激光烧结先驱体浸渍裂解
Keywords:
 Keywords:ceramic composite additive manufacturing selective laser sintering precursor impregnation and pyrolysis
分类号:
TB332
DOI:
10.15938/j.jhust.2020.03.025
文献标志码:
A
摘要:
 摘要:针对选择性激光烧结技术(SLS)成型陶瓷材料致密性低、力学性能差的问题,采用选择性激光烧结技术(SLS)与聚合物浸渍裂解技术(PIP)相结合的方法,以碳化硅、环氧树脂和聚碳硅烷为原料,制备SiC/SiC陶瓷基复合材料。研究选择性激光烧结工艺参数、试件尺寸精度、微观结构及弯曲性能。结果表明:通过SLS/PIP技术可有效降低碳化硅陶瓷试件的孔隙率,试件密度为245 g/cm3,弯曲强度达到13828 MPa。该方法可以实现传统方法无法解决的表面及内部复杂结构碳化硅陶瓷基复合材料的制备问题。
Abstract:
Abstract:In order to improve the density and mechanical property of ceramics fabricated by selective laser sintering (SLS) process, a new method that combined SLS with precursor impregnation and pyrolysis (PIP) process was presented to fabricated silicon carbide particulate/silicon carbide matrix (SiC/SiC) ceramic composites Starting with SiC powders of 17~70 μm sizes, the preform was produced by printing epoxy binder To gain the dense composites, the SiC preforms were infiltrated with polycarbosilane liquid and pyrolyzed at 1200℃ under nitrogen atmosphere for 8 repeated cycles The porosity of the specimen greatly decreased and the density reached to 245 g/cm3 after PIP process Analysis of results and discussions of optimum printing parameters, dimension accuracy, microstructure and bending strength for SiC/SiC composites are also presented The mechanical property of the SiC/SiC composite fabricated by SLS/PIP process has been improved and its bending strength attained 13828 MPa In addition, the netshape silicon carbide components with complex surface and inner structure were fabricated

参考文献/References:

 [1]GAN Ke, XU Jie, LU Yuju, et al. Preparation of Silicon Carbide Ceramics Using Chemical Treated Powder by DCC Via Dispersant Reaction and Liquid Phase Sintering[J]. Journal of the European Ceramic Society, 2017, 37(3): 891.
[2]SANTOS A C, RIBEIRO S. Liquid Phase Sintering and Characterization of SiC Ceramics[J]. Ceramics International, 2018, 44(10): 11048. 
[3]EDWARDS D P, MUDDLE B C, CHENG Yibing, et al. The Development of Microstructure in Silicon NitrideBonded Silicon Carbide[J]. Journal of the European Ceramic Society, 1995, 15(5):415.
[4]ZHANG Jingxian, JIANG Dongliang, LIN Qingling, et al. Properties of Silicon Carbide Ceramics from Gelcasting and Pressureless Sintering[J]. Materials & Design (1980-2015), 2015, 65: 12. 
[5]BLACKBURN S. New Processes or Old: Complex Shape Processing of Advanced Ceramics[J]. Advances in applied ceramics, 2005, 104(3): 97. 
[6]HON K K B, GILL T J. Selective Laser Sintering of SiC/Polyamide Composites[J]. CIRP Annals, 2003, 52(1): 173.
[7]DANEZAN A, DELAIZIR G, TESSIERDOYEN N, et al. Selective Laser Sintering of Porcelain[J]. Journal of the European Ceramic Society, 2018, 38(2): 769.
[8]ZHU Wei, YAN Chunze, SHI Yunsong, et al. Investigation into Mechanical and Microstructural Properties of Polypropylene Manufactured by Selective Laser Sintering in Comparison with Injection Molding Counterparts[J]. Materials & Design, 2015, 82: 37.
[9]XIE Fangxia, HE Xinbo, CAO Shunli, et al. Structural and Mechanical Characteristics of Porous 316L Stainless Steel Fabricated by Indirect Selective Laser Sintering[J]. Journal of Materials Processing Technology, 2013, 213(6): 838.
[10]NELSON J C, VAIL N K, BARLOW J W, et al. Selective Laser Sintering of PolymerCoated Silicon Carbide Powders[J]. Industrial & Engineering Chemistry Research, 1995, 34(5): 1641.
[11]GILL T J, HON K K B. Experimental Investigation into the Selective Laser Sintering of Silicon Carbide Polyamide Composites[J]. Proceedings of the Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, 2004, 218(10): 1249.
[12]SHAHZAD K, DECKERS J, BOURY S, et al. Preparation and Indirect Selective Laser Sintering of Alumina/PA Microspheres[J]. Ceramics International, 2012, 38(2): 1241.
[13]XIONG Bowen, YU Huan, XU Zhifeng, et al. Study on Dual Binders for Fabricating SiC Particulate Preforms Using Selective Laser Sintering[J]. Composites Part B: Engineering, 2013, 48: 129.
[14]CHEN Annan, WU Jiamin, LIU Kai, et al. Highperformance Ceramic Parts with Complex Shape Prepared by Selective Laser Sintering: A Review[J]. Advances in Applied Ceramics, 2018, 117(2): 100.
[15]WANG Zijian, SHI Yusheng, HE Wenting, et al. Compound Process of Selective Laser Processed Alumina Parts Densified by Cold Isostatic Pressing and Solid State Sintering: Experiments, Full Process Simulation and Parameter Optimization[J]. Ceramics International, 2015, 41(2): 3245.
[16]LIU Kai, SUN Huajun, SHI Yusheng, et al. Research on Selective Laser Sintering of KaolinEpoxy Resin Ceramic Powders Combined with Cold Isostatic Pressing and Sintering[J]. Ceramics International, 2016, 42(9): 10711.
[17]FRIEDEL T, TRAVITZKY N, NIEBLING F, et al. Fabrication of Polymer Derived Ceramic Parts by Selective Laser Curing[J]. Journal of the European Ceramic Society, 2005, 25(2/3): 193.
[18]SUBRAMANIAN K, VAIL N, BARLOW J, et al. Selective Laser Sintering of Alumina with Polymer Binders[J]. Rapid Prototyping Journal, 1995, 1(2): 24.
[19]EVANS R S, BOURELL D L, BEAMAN J J, et al. Rapid Manufacturing of Silicon Carbide Composites[J]. Rapid Prototyping Journal, 2005, 11(1): 37.
[20]LI Guangde, ZHANG Changrui, HU Haifeng, et al. Preparation and Mechanical Properties of C/SiC Nuts and Bolts[J]. Materials Science and Engineering: A, 2012, 547: 1.
[21]LY H Q, TAYLOR R, DAY R J. Carbon FibreReinforced CMCs by PCS Infiltration[J]. Journal of materials science, 2001, 36(16): 4027.
[22]LIU Kai, SHI Yusheng, LI Chenhui, et al. Indirect Selective Laser Sintering of Epoxy ResinAl2O3 Ceramic Powders Combined with Cold Isostatic Pressing[J]. Ceramics International, 2014, 40(5): 7099.
[23]马丽君, 李文凤, 黄庆飞, 等. Si粉粒径及其添加量对SiC陶瓷材料结构和性能的影响[J]. 金刚石与磨料磨具工程, 2018, 38(4): 61.
MA Lijun, LI Wenfeng, HUANG Qingfei, et al. Effect of Particle Size and Content of Silicon Powder on Microstructure and Properties of SiC Ceramic Materials[J]. Diamond & Abrasives Engineering, 2018, 38(4): 61.
[24]陈鹏, 朱小刚, 吴甲民, 等. 基于SLS/CIP工艺SiC陶瓷的制备及其性能[J]. 材料工程, 2019, 47(3): 87.
CHEN Peng, ZHU Xiaogang, WU Jiamin, et al. Preparation and Properties of SiC Ceramics Via SLS/CIP Process[J]. Journal of Materials Engineering, 2019, 47(3): 87.

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备注/Memo

备注/Memo:
 收稿日期: 2018-10-25
基金项目: 国家自然科学基金(11432005).
作者简介:
周义凯(1993—),男,硕士;
张坤(1982—),女,博士研究生,讲师
通信作者:
曾涛(1967—),男,教授,博士研究生导师,Email:taozeng@hrbust.edu.cn
更新日期/Last Update: 2020-10-14